Transmetalation of Aqueous Inorganic Clusters: A Useful Route to the Synthesis of Heterometallic Aluminum and Indium Hydroxo-Aquo Clusters.
Identifieur interne : 000019 ( Main/Exploration ); précédent : 000018; suivant : 000020Transmetalation of Aqueous Inorganic Clusters: A Useful Route to the Synthesis of Heterometallic Aluminum and Indium Hydroxo-Aquo Clusters.
Auteurs : RBID : pubmed:24742048Abstract
[AlxIny(μ3-OH)6(μ-OH)18(H2O)24](NO3)15 hydroxy-aquo clusters (AlxIn13-x) are synthesized through the evaporation of stoichiometrically varied solutions of Al13 and In(NO3)3 using a transmetalation reaction. Several spectroscopic techniques ((1)H NMR, (1)H-diffusion ordered spectroscopy, dynamic light scattering, and Raman) are used to compare AlxIn13-x to its Al13 counterpart. A thin film of aluminum indium oxide was prepared from an Al7In6 cluster ink, showing its utility as a precursor for materials.
DOI: 10.1021/ic403121r
PubMed: 24742048
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<record><TEI><teiHeader><fileDesc><titleStmt><title xml:lang="en">Transmetalation of Aqueous Inorganic Clusters: A Useful Route to the Synthesis of Heterometallic Aluminum and Indium Hydroxo-Aquo Clusters.</title><author><name sortKey="Kamunde Devonish, Maisha K" uniqKey="Kamunde Devonish M">Maisha K Kamunde-Devonish</name><affiliation wicri:level="1"><nlm:affiliation>Department of Chemistry & Biochemistry and Materials Science Institute, University of Oregon , Eugene, Oregon 97403-1253, United States.</nlm:affiliation><country xml:lang="fr">États-Unis</country><wicri:regionArea>Department of Chemistry & Biochemistry and Materials Science Institute, University of Oregon , Eugene, Oregon 97403-1253</wicri:regionArea></affiliation></author><author><name sortKey="Jackson, Milton N" uniqKey="Jackson M">Milton N Jackson</name></author><author><name sortKey="Mensinger, Zachary L" uniqKey="Mensinger Z">Zachary L Mensinger</name></author><author><name sortKey="Zakharov, Lev N" uniqKey="Zakharov L">Lev N Zakharov</name></author><author><name sortKey="Johnson, Darren W" uniqKey="Johnson D">Darren W Johnson</name></author></titleStmt><publicationStmt><date when="2014">2014</date><idno type="doi">10.1021/ic403121r</idno><idno type="RBID">pubmed:24742048</idno><idno type="pmid">24742048</idno><idno type="wicri:Area/Main/Corpus">000053</idno><idno type="wicri:Area/Main/Curation">000053</idno><idno type="wicri:Area/Main/Exploration">000019</idno></publicationStmt></fileDesc><profileDesc><textClass></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">[AlxIny(μ3-OH)6(μ-OH)18(H2O)24](NO3)15 hydroxy-aquo clusters (AlxIn13-x) are synthesized through the evaporation of stoichiometrically varied solutions of Al13 and In(NO3)3 using a transmetalation reaction. Several spectroscopic techniques ((1)H NMR, (1)H-diffusion ordered spectroscopy, dynamic light scattering, and Raman) are used to compare AlxIn13-x to its Al13 counterpart. A thin film of aluminum indium oxide was prepared from an Al7In6 cluster ink, showing its utility as a precursor for materials.</div></front></TEI><pubmed><MedlineCitation Status="Publisher" Owner="NLM"><PMID Version="1">24742048</PMID><DateCreated><Year>2014</Year><Month>4</Month><Day>18</Day></DateCreated><Article PubModel="Print-Electronic"><Journal><ISSN IssnType="Electronic">1520-510X</ISSN><JournalIssue CitedMedium="Internet"><PubDate><Year>2014</Year><Month>Apr</Month><Day>18</Day></PubDate></JournalIssue><Title>Inorganic chemistry</Title><ISOAbbreviation>Inorg Chem</ISOAbbreviation></Journal><ArticleTitle>Transmetalation of Aqueous Inorganic Clusters: A Useful Route to the Synthesis of Heterometallic Aluminum and Indium Hydroxo-Aquo Clusters.</ArticleTitle><Pagination><MedlinePgn></MedlinePgn></Pagination><Abstract><AbstractText NlmCategory="UNLABELLED">[AlxIny(μ3-OH)6(μ-OH)18(H2O)24](NO3)15 hydroxy-aquo clusters (AlxIn13-x) are synthesized through the evaporation of stoichiometrically varied solutions of Al13 and In(NO3)3 using a transmetalation reaction. Several spectroscopic techniques ((1)H NMR, (1)H-diffusion ordered spectroscopy, dynamic light scattering, and Raman) are used to compare AlxIn13-x to its Al13 counterpart. A thin film of aluminum indium oxide was prepared from an Al7In6 cluster ink, showing its utility as a precursor for materials.</AbstractText></Abstract><AuthorList><Author><LastName>Kamunde-Devonish</LastName><ForeName>Maisha K</ForeName><Initials>MK</Initials><Affiliation>Department of Chemistry & Biochemistry and Materials Science Institute, University of Oregon , Eugene, Oregon 97403-1253, United States.</Affiliation></Author><Author><LastName>Jackson</LastName><ForeName>Milton N</ForeName><Initials>MN</Initials><Suffix>Jr</Suffix></Author><Author><LastName>Mensinger</LastName><ForeName>Zachary L</ForeName><Initials>ZL</Initials></Author><Author><LastName>Zakharov</LastName><ForeName>Lev N</ForeName><Initials>LN</Initials></Author><Author><LastName>Johnson</LastName><ForeName>Darren W</ForeName><Initials>DW</Initials></Author></AuthorList><Language>ENG</Language><PublicationTypeList><PublicationType>JOURNAL ARTICLE</PublicationType></PublicationTypeList><ArticleDate DateType="Electronic"><Year>2014</Year><Month>4</Month><Day>18</Day></ArticleDate></Article><MedlineJournalInfo><MedlineTA>Inorg Chem</MedlineTA><NlmUniqueID>0366543</NlmUniqueID><ISSNLinking>0020-1669</ISSNLinking></MedlineJournalInfo></MedlineCitation><PubmedData><History><PubMedPubDate PubStatus="entrez"><Year>2014</Year><Month>4</Month><Day>19</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate><PubMedPubDate PubStatus="pubmed"><Year>2014</Year><Month>4</Month><Day>20</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate><PubMedPubDate PubStatus="medline"><Year>2014</Year><Month>4</Month><Day>20</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate></History><PublicationStatus>aheadofprint</PublicationStatus><ArticleIdList><ArticleId IdType="doi">10.1021/ic403121r</ArticleId><ArticleId IdType="pubmed">24742048</ArticleId></ArticleIdList></PubmedData></pubmed></record>Pour manipuler ce document sous Unix (Dilib)
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